The GLM Procedure
      Class Level Information
Class         Levels    Values
sample             6    1 2 3 4 5 6 
tissue             2    flo veg     
Number of observations    12
The GLM Procedure
Dependent Variable: conc1   
                                      Sum of
Source                     DF        Squares    Mean Square   F Value   Pr > F
Model                       6    28.01059667     4.66843278      3.01   0.1233
Error                       5     7.74841300     1.54968260                   
Corrected Total            11    35.75900967                                  
R-Square     Coeff Var      Root MSE    conc1 Mean
0.783316      15.44271      1.244862      8.061167
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
sample                      5     2.02684967     0.40536993      0.26   0.9163
tissue                      1    25.98374700    25.98374700     16.77   0.0094
The GLM Procedure
Dependent Variable: conc2   
                                      Sum of
Source                     DF        Squares    Mean Square   F Value   Pr > F
Model                       6     9.45368150     1.57561358      1.15   0.4494
Error                       5     6.86250742     1.37250148                   
Corrected Total            11    16.31618892                                  
R-Square     Coeff Var      Root MSE    conc2 Mean
0.579405      16.15228      1.171538      7.253083
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
sample                      5     6.38832942     1.27766588      0.93   0.5304
tissue                      1     3.06535208     3.06535208      2.23   0.1953
The GLM Procedure
Dependent Variable: conc3   
                                      Sum of
Source                     DF        Squares    Mean Square   F Value   Pr > F
Model                       6    15.03615900     2.50602650      2.97   0.1263
Error                       5     4.21949367     0.84389873                   
Corrected Total            11    19.25565267                                  
R-Square     Coeff Var      Root MSE    conc3 Mean
0.780870      11.87845      0.918640      7.733667
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
sample                      5    10.36863767     2.07372753      2.46   0.1731
tissue                      1     4.66752133     4.66752133      5.53   0.0654
The GLM Procedure
Dependent Variable: conc4   
                                      Sum of
Source                     DF        Squares    Mean Square   F Value   Pr > F
Model                       6    13.53428300     2.25571383     17.14   0.0034
Error                       5     0.65808867     0.13161773                   
Corrected Total            11    14.19237167                                  
R-Square     Coeff Var      Root MSE    conc4 Mean
0.953631      4.528574      0.362792      8.011167
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
sample                      5     6.65163767     1.33032753     10.11   0.0120
tissue                      1     6.88264533     6.88264533     52.29   0.0008
The GLM Procedure
Dependent Variable: conc5   
                                      Sum of
Source                     DF        Squares    Mean Square   F Value   Pr > F
Model                       6    16.30054950     2.71675825      4.59   0.0578
Error                       5     2.95880342     0.59176068                   
Corrected Total            11    19.25935292                                  
R-Square     Coeff Var      Root MSE    conc5 Mean
0.846371      8.872748      0.769260      8.669917
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
sample                      5     6.98837942     1.39767588      2.36   0.1836
tissue                      1     9.31217008     9.31217008     15.74   0.0107
The GLM Procedure
Dependent Variable: conc6   
                                      Sum of
Source                     DF        Squares    Mean Square   F Value   Pr > F
Model                       6     6.13200400     1.02200067      3.11   0.1166
Error                       5     1.64084000     0.32816800                   
Corrected Total            11     7.77284400                                  
R-Square     Coeff Var      Root MSE    conc6 Mean
0.788901      6.118986      0.572859      9.362000
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
sample                      5     5.89003600     1.17800720      3.59   0.0935
tissue                      1     0.24196800     0.24196800      0.74   0.4298
The GLM Procedure
Dependent Variable: conc7   
                                      Sum of
Source                     DF        Squares    Mean Square   F Value   Pr > F
Model                       6    20.08224467     3.34704078      2.24   0.1977
Error                       5     7.48770500     1.49754100                   
Corrected Total            11    27.56994967                                  
R-Square     Coeff Var      Root MSE    conc7 Mean
0.728411      11.54019      1.223741      10.60417
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
sample                      5    17.32320167     3.46464033      2.31   0.1893
tissue                      1     2.75904300     2.75904300      1.84   0.2327
The GLM Procedure
Repeated Measures Analysis of Variance
                    Repeated Measures Level Information
Dependent Variable       conc1    conc2    conc3    conc4    conc5    conc6
   Level of julian         179      200      221      242      269      290
       Repeated Measures
       Level Information
Dependent Variable       conc7
   Level of julian         320
The GLM Procedure
Repeated Measures Analysis of Variance
Tests of Hypotheses for Between Subjects Effects
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
sample                      5     6.84272367     1.36854473      1.31   0.3870
tissue                      1    35.90198876    35.90198876     34.38   0.0020
Error                       5     5.22202152     1.04440430                   
The GLM Procedure
Repeated Measures Analysis of Variance
Univariate Tests of Hypotheses for Within Subject Effects
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
julian                      6    93.21110731    15.53518455     17.68   <.0001
julian*sample              30    48.79434783     1.62647826      1.85   0.0484
julian*tissue               6    17.01045807     2.83507635      3.23   0.0144
Error(julian)              30    26.35382964     0.87846099                   
                          Adj Pr > F
Source                  G - G     H - F
julian                 <.0001    <.0001
julian*sample          0.1316    0.0484
julian*tissue          0.0581    0.0144
Error(julian)                          
Greenhouse-Geisser Epsilon    0.4631
Huynh-Feldt Epsilon           2.3515
The GLM Procedure
Least Squares Means
tissue  conc1 LSMEAN  conc2 LSMEAN  conc3 LSMEAN  conc4 LSMEAN  conc5 LSMEAN
flo       6.58966667    6.74766667    7.11000000    7.25383333    7.78900000
veg       9.53266667    7.75850000    8.35733333    8.76850000    9.55083333
tissue  conc6 LSMEAN    conc7 LSMEAN
flo       9.50400000      10.1246667
veg       9.22000000      11.0836667
               Plot of LSMEAN*julian.  Symbol is value of tissue.
LSMEAN |
       |
  11.5 +
       |
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  11.0 +
       |
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  10.5 +
       |
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       |
       |                                                                      f
  10.0 +
       |
       |
       |
       |                                             v
   9.5 +     v                                                 f
       |
       |
       |                                                       v
       |
   9.0 +
       |
       |                                    v
       |
       |
   8.5 +
       |                          v
       |
       |
       |
   8.0 +
       |
       |               v                             f
       |
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   7.5 +
       |
       |                                    f
       |
       |                          f
   7.0 +
       |
       |
       |               f
       |     f
   6.5 +
       |
       -+---------+---------+---------+---------+---------+---------+---------+-
       180       200       220       240       260       280       300       320
                                         julian
The GLM Procedure
    Class Level Information
Class         Levels    Values
tissue             2    flo veg 
Number of observations    12
The GLM Procedure
Repeated Measures Analysis of Variance
                    Repeated Measures Level Information
Dependent Variable       conc1    conc2    conc3    conc4    conc5    conc6
   Level of julian         179      200      221      242      269      290
       Repeated Measures
       Level Information
Dependent Variable       conc7
   Level of julian         320
  Partial Correlation Coefficients from the Error SSCP Matrix / Prob > |r|
DF = 10     conc1     conc2     conc3     conc4     conc5     conc6     conc7
conc1    1.000000  0.134474  0.041460 -0.043679  0.362419  0.103922 -0.314957
                     0.6934    0.9037    0.8985    0.2734    0.7611    0.3455
conc2    0.134474  1.000000  0.447446 -0.534294  0.059159 -0.305750 -0.351114
           0.6934              0.1676    0.0904    0.8628    0.3605    0.2897
conc3    0.041460  0.447446  1.000000 -0.629701 -0.290414 -0.409596 -0.136772
           0.9037    0.1676              0.0379    0.3863    0.2109    0.6884
conc4   -0.043679 -0.534294 -0.629701  1.000000  0.587425  0.365034  0.274047
           0.8985    0.0904    0.0379              0.0574    0.2697    0.4148
conc5    0.362419  0.059159 -0.290414  0.587425  1.000000  0.467132  0.003847
           0.2734    0.8628    0.3863    0.0574              0.1474    0.9910
conc6    0.103922 -0.305750 -0.409596  0.365034  0.467132  1.000000  0.480414
           0.7611    0.3605    0.2109    0.2697    0.1474              0.1347
conc7   -0.314957 -0.351114 -0.136772  0.274047  0.003847  0.480414  1.000000
           0.3455    0.2897    0.6884    0.4148    0.9910    0.1347          
                             E = Error SSCP Matrix
       julian_N represents the nth degree polynomial contrast for julian
            julian_1    julian_2    julian_3    julian_4    julian_5    julian_6
julian_1    27.39687     6.02920     0.16131     7.86022    -2.10884    -7.69737
julian_2     6.02920     7.77943     2.25399     0.48694    -2.43576    -0.22756
julian_3     0.16131     2.25399    15.51495    -4.92731    -2.80410     5.26278
julian_4     7.86022     0.48694    -4.92731     9.76926    -0.95689    -4.21350
julian_5    -2.10884    -2.43576    -2.80410    -0.95689     6.64213    -2.48450
julian_6    -7.69737    -0.22756     5.26278    -4.21350    -2.48450     8.04554
The GLM Procedure
Repeated Measures Analysis of Variance
       Partial Correlation Coefficients from the Error SSCP Matrix of the
         Variables Defined by the Specified Transformation / Prob > |r|
DF = 10     julian_1    julian_2    julian_3    julian_4    julian_5    julian_6
julian_1    1.000000    0.412986    0.007824    0.480456   -0.156329   -0.518459
                          0.2068      0.9818      0.1347      0.6462      0.1023
julian_2    0.412986    1.000000    0.205165    0.055856   -0.338850   -0.028763
              0.2068                  0.5451      0.8704      0.3080      0.9331
julian_3    0.007824    0.205165    1.000000   -0.400225   -0.276226    0.471045
              0.9818      0.5451                  0.2226      0.4109      0.1436
julian_4    0.480456    0.055856   -0.400225    1.000000   -0.118789   -0.475264
              0.1347      0.8704      0.2226                  0.7279      0.1396
julian_5   -0.156329   -0.338850   -0.276226   -0.118789    1.000000   -0.339866
              0.6462      0.3080      0.4109      0.7279                  0.3065
julian_6   -0.518459   -0.028763    0.471045   -0.475264   -0.339866    1.000000
              0.1023      0.9331      0.1436      0.1396      0.3065            
                            Sphericity Tests
                                   Mauchly's
Variables                    DF    Criterion    Chi-Square    Pr > ChiSq
Transformed Variates         20    0.0669579     21.028714        0.3954
Orthogonal Components        20    0.0669579     21.028714        0.3954
                  Manova Test Criteria and Exact F Statistics
                     for the Hypothesis of no julian Effect
                      H = Type III SSCP Matrix for julian
                             E = Error SSCP Matrix
                              S=1    M=2    N=1.5
Statistic                        Value    F Value    Num DF    Den DF    Pr > F
Wilks' Lambda               0.13063553       5.55         6         5    0.0400
Pillai's Trace              0.86936447       5.55         6         5    0.0400
Hotelling-Lawley Trace      6.65488518       5.55         6         5    0.0400
Roy's Greatest Root         6.65488518       5.55         6         5    0.0400
The GLM Procedure
Repeated Measures Analysis of Variance
                Manova Test Criteria and Exact F Statistics for
                   the Hypothesis of no julian*tissue Effect
                   H = Type III SSCP Matrix for julian*tissue
                             E = Error SSCP Matrix
                              S=1    M=2    N=1.5
Statistic                        Value    F Value    Num DF    Den DF    Pr > F
Wilks' Lambda               0.21166956       3.10         6         5    0.1173
Pillai's Trace              0.78833044       3.10         6         5    0.1173
Hotelling-Lawley Trace      3.72434493       3.10         6         5    0.1173
Roy's Greatest Root         3.72434493       3.10         6         5    0.1173
The GLM Procedure
Repeated Measures Analysis of Variance
Tests of Hypotheses for Between Subjects Effects
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
tissue                      1    35.90198876    35.90198876     29.76   0.0003
Error                      10    12.06474519     1.20647452                   
The GLM Procedure
Repeated Measures Analysis of Variance
Univariate Tests of Hypotheses for Within Subject Effects
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
julian                      6    93.21110731    15.53518455     12.40   <.0001
julian*tissue               6    17.01045807     2.83507635      2.26   0.0491
Error(julian)              60    75.14817748     1.25246962                   
                          Adj Pr > F
Source                  G - G     H - F
julian                 <.0001    <.0001
julian*tissue          0.0968    0.0577
Error(julian)                          
Greenhouse-Geisser Epsilon    0.5312
Huynh-Feldt Epsilon           0.8868
The GLM Procedure
Repeated Measures Analysis of Variance
Analysis of Variance of Contrast Variables
julian_N represents the nth degree polynomial contrast for julian
Contrast Variable: julian_1            
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
Mean                        1    73.71945589    73.71945589     26.91   0.0004
tissue                      1     6.44455483     6.44455483      2.35   0.1561
Error                      10    27.39687345     2.73968734                   
Contrast Variable: julian_2            
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
Mean                        1    16.53994026    16.53994026     21.26   0.0010
tissue                      1     1.06560438     1.06560438      1.37   0.2690
Error                      10     7.77942893     0.77794289                   
Contrast Variable: julian_3            
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
Mean                        1     1.18002159     1.18002159      0.76   0.4036
tissue                      1     0.32201707     0.32201707      0.21   0.6584
Error                      10    15.51494771     1.55149477                   
Contrast Variable: julian_4            
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
Mean                        1     1.04190309     1.04190309      1.07   0.3261
tissue                      1     7.62108321     7.62108321      7.80   0.0190
Error                      10     9.76925736     0.97692574                   
Contrast Variable: julian_5            
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
Mean                        1     0.55166841     0.55166841      0.83   0.3836
tissue                      1     0.99066582     0.99066582      1.49   0.2500
Error                      10     6.64213326     0.66421333                   
The GLM Procedure
Repeated Measures Analysis of Variance
Analysis of Variance of Contrast Variables
julian_N represents the nth degree polynomial contrast for julian
Contrast Variable: julian_6            
Source                     DF    Type III SS    Mean Square   F Value   Pr > F
Mean                        1     0.17811808     0.17811808      0.22   0.6481
tissue                      1     0.56653276     0.56653276      0.70   0.4210
Error                      10     8.04553677     0.80455368                   
The GLM Procedure
Least Squares Means
tissue  conc1 LSMEAN  conc2 LSMEAN  conc3 LSMEAN  conc4 LSMEAN  conc5 LSMEAN
flo       6.58966667    6.74766667    7.11000000    7.25383333    7.78900000
veg       9.53266667    7.75850000    8.35733333    8.76850000    9.55083333
tissue  conc6 LSMEAN    conc7 LSMEAN
flo       9.50400000      10.1246667
veg       9.22000000      11.0836667
The Mixed Procedure
                  Model Information
Data Set                     WORK.CONCS               
Dependent Variable           conc                     
Covariance Structure         Variance Components      
Estimation Method            REML                     
Residual Variance Method     Profile                  
Fixed Effects SE Method      Model-Based              
Degrees of Freedom Method    Containment              
             Class Level Information
Class     Levels    Values
tissue         2    flo veg                       
sample         6    1 2 3 4 5 6                   
wp            12    1 2 3 4 5 6 7 8 9 10 11 12    
date           7    179 200 221 242 269 290 320   
            Dimensions
Covariance Parameters             3
Columns in X                     24
Columns in Z                     18
Subjects                          1
Max Obs Per Subject              84
Observations Used                84
Observations Not Used             0
Total Observations               84
                     Iteration History
Iteration    Evaluations    -2 Res Log Like       Criterion
        0              1       239.12603637                
        1              3       239.10235984      0.00001750
        2              2       239.10142005      0.00000003
        3              1       239.10141850      0.00000000
                   Convergence criteria met.                    
   Covariance Parameter
        Estimates
Cov Parm          Estimate
sample            0.009434
tissue*sample            0
Residual            1.2365
           Fitting Information
Res Log Likelihood                  -119.6
Akaike's Information Criterion      -121.6
The Mixed Procedure
           Fitting Information
Schwarz's Bayesian Criterion        -121.3
-2 Res Log Likelihood                239.1
         Type 3 Tests of Fixed Effects
                Num     Den
Effect           DF      DF    F Value    Pr > F
tissue            1       5      29.04    0.0030
date              6      60      12.56    <.0001
tissue*date       6      60       2.29    0.0465
The Mixed Procedure
                  Model Information
Data Set                     WORK.CONCS               
Dependent Variable           conc                     
Covariance Structures        Variance Components,     
                             Compound Symmetry        
Subject Effect               tissue*sample            
Estimation Method            REML                     
Residual Variance Method     Profile                  
Fixed Effects SE Method      Model-Based              
Degrees of Freedom Method    Containment              
             Class Level Information
Class     Levels    Values
tissue         2    flo veg                       
sample         6    1 2 3 4 5 6                   
wp            12    1 2 3 4 5 6 7 8 9 10 11 12    
date           7    179 200 221 242 269 290 320   
            Dimensions
Covariance Parameters             3
Columns in X                     24
Columns in Z                      6
Subjects                          1
Max Obs Per Subject              84
Observations Used                84
Observations Not Used             0
Total Observations               84
                     Iteration History
Iteration    Evaluations    -2 Res Log Like       Criterion
        0              1       239.12603637                
        1              1       239.02903841      0.00000000
                   Convergence criteria met.                    
    Covariance Parameter Estimates
Cov Parm     Subject          Estimate
sample                         0.02315
CS           tissue*sample    -0.02972
Residual                        1.2525
           Fitting Information
Res Log Likelihood                  -119.5
Akaike's Information Criterion      -122.5
Schwarz's Bayesian Criterion        -122.2
The Mixed Procedure
           Fitting Information
-2 Res Log Likelihood                239.0
         Type 3 Tests of Fixed Effects
                Num     Den
Effect           DF      DF    F Value    Pr > F
tissue            1      65      34.38    <.0001
date              6      65      12.40    <.0001
tissue*date       6      65       2.26    0.0480
                             Least Squares Means
                                         Standard
Effect        tissue   date   Estimate      Error     DF   t Value   Pr > |t|
tissue*date   flo      179      6.5897     0.4557     65     14.46     <.0001
tissue*date   flo      200      6.7477     0.4557     65     14.81     <.0001
tissue*date   flo      221      7.1100     0.4557     65     15.60     <.0001
tissue*date   flo      242      7.2538     0.4557     65     15.92     <.0001
tissue*date   flo      269      7.7890     0.4557     65     17.09     <.0001
tissue*date   flo      290      9.5040     0.4557     65     20.86     <.0001
tissue*date   flo      320     10.1247     0.4557     65     22.22     <.0001
tissue*date   veg      179      9.5327     0.4557     65     20.92     <.0001
tissue*date   veg      200      7.7585     0.4557     65     17.03     <.0001
tissue*date   veg      221      8.3573     0.4557     65     18.34     <.0001
tissue*date   veg      242      8.7685     0.4557     65     19.24     <.0001
tissue*date   veg      269      9.5508     0.4557     65     20.96     <.0001
tissue*date   veg      290      9.2200     0.4557     65     20.23     <.0001
tissue*date   veg      320     11.0837     0.4557     65     24.32     <.0001
The Mixed Procedure
                  Model Information
Data Set                     WORK.CONCS               
Dependent Variable           conc                     
Covariance Structures        Variance Components,     
                             Compound Symmetry        
Subject Effect               tissue*sample            
Estimation Method            REML                     
Residual Variance Method     Profile                  
Fixed Effects SE Method      Model-Based              
Degrees of Freedom Method    Containment              
             Class Level Information
Class     Levels    Values
tissue         2    flo veg                       
sample         6    1 2 3 4 5 6                   
wp            12    1 2 3 4 5 6 7 8 9 10 11 12    
            Dimensions
Covariance Parameters             3
Columns in X                     12
Columns in Z                      6
Subjects                          1
Max Obs Per Subject              84
Observations Used                84
Observations Not Used             0
Total Observations               84
                     Iteration History
Iteration    Evaluations    -2 Res Log Like       Criterion
        0              1       355.44511765                
        1              1       355.32806426      0.00000000
                   Convergence criteria met.                    
    Covariance Parameter Estimates
Cov Parm     Subject          Estimate
sample                         0.02315
CS           tissue*sample    -0.03716
Residual                        1.3045
           Fitting Information
Res Log Likelihood                  -177.7
Akaike's Information Criterion      -180.7
Schwarz's Bayesian Criterion        -180.4
-2 Res Log Likelihood                355.3
The Mixed Procedure
              Type 3 Tests of Fixed Effects
                         Num     Den
Effect                    DF      DF    F Value    Pr > F
tissue                     1      71       0.51    0.4761
date                       1      71       1.57    0.2143
date*tissue                1      71       0.37    0.5454
date*date                  1      71       1.28    0.2610
date*date*tissue           1      71       0.29    0.5890
date*date*date             1      71       1.05    0.3094
date*date*date*tissu       1      71       0.25    0.6208
